Welcome to the Amira-Avizo Software Use Case Gallery

Porous binary Ti-10Mo alloys were prepared using non-spherical titanium, molybdenum powders by the powder metallurgy (PM) space holder technique. Based on the three-dimensional analysis of porosity characteristics, a detailed assessment of the effects of porosity on mechanical properties and corrosion resistances in phosphate-buffered saline (PBS) was carried out. For comparison, PM-fabricated CP-Ti with 50.5% porosity sintered at 1200 °C for 2 h and dense Ti-10Mo alloy sintered at 1450 °C ... Read more

Laser-matter interactions in laser additive manufacturing (LAM) occur on short time scales (10^-6 – 10^-3 s) and have traditionally proven difficult to characterise. We investigate these interactions during LAM of stainless steel (SS316 L) and 13-93 bioactive glass powders using a custom built LAM process replicator (LAMPR) with in situ and operando synchrotron X-ray radiography. This reveals a range of melt track solidification phenomena as... Read more

Dense calcium caseinate dispersions can be transformed into hierarchically fibrous structures by shear deformation. This transformation can be attributed to the intrinsic properties of calcium caseinate. Depending on the dispersion preparation method, a certain amount of air gets entrapped in the sheared protein matrix. Although anisotropy is obtained in the absence of entrapped air, the fibrous appearance and mechanical anisotropy of the calcium caseinate materials are more pronounced with... Read more

The near-threshold behavior of long cracks is evaluated using pre-cracked flat dogbone specimens of a commercial aluminum alloy in two heat treatment states. Once the threshold was known, the crack initially introduced by cyclic compression was propagated under load control with approximately
constant range of the stress intensity factor at values close to the threshold values. The 3D morphology of the crack and the spatial distribution of the primary precipitates obtained by µ-CT were... Read more

The effect of the defect size and morphology on the fatigue damage evolution was analysed in a recycled Al-Si-Cu alloy by micro-computed tomography and scanning electron microscopy. Fatigue tests were performed and the different crack initiation scenarios were characterized and classified. The interaction between shrinkage and gas pores was the key crack initiation mechanism and the ß-Al5FeSi particles did not play any role in the crack initiation phase. However, crack path analysis indicate... Read more

The flow distribution behaviour of open-cell metallic foam fuel cell flow-fields are evaluated using ex-situ optical analysis and X-ray computed tomography (X-ray CT). Five different manifold designs are evaluated and flow distribution and pressure drop ... Read more

In this study, chemically bonded phosphate ceramic (CBPC) fiber reinforced composites were made at indoor temperatures. The mechanical properties and microstructure of the CBPC composites were studied. The CBPC matrix of aluminum phosphate binder, metakaolin, and magnesia with different Si/P ratios was prepared. The results show that when the Si/P ratio was 1.2, and magnesia content in the CBPC was 15%, CBPC reached its maximum flexural strength. The fiber reinforced CBPC composites were prep... Read more

We have experimentally investigated the impact of heterogeneity on the dissolution of two limestones, characterised by distinct degrees of flow heterogeneity at both the pore and core scales. The two rocks were reacted with reservoir-condition CO₂-saturated brine at both scales and scanned dynamically during dissolution. First, 1 cm long 4 mm... Read more

We introduce the application of microbial-induced calcite precipitation via the ureolytic soil bacterium Sporosarcina Pasteurii in freeze-dried form, as a means of enhancing overall MICP efficiency and reproducibility for geotechnical engineering applications. We show that the execution of urea hydrolysis and CaCO₃ precipitation persist as a “cell-free” mechanism upon the complete breakdown of rehydrated cell clusters. Further, strength and stiffness parameters of bio-cemented ... Read more

Electrospun constructs for the repair of load-bearing tissues are required to have adequate mechanical properties. However, the failure mechanisms of electrospun fibrous materials are not well understood. Existing literature focuses on failure modes of individual fibers and/or on bulk mechanical properties of whole fiber mats.

Electrospinning allows the production of fibrous networks for tissue engineering, drug delivery, and wound healing in health care. It enables the production of c... Read more

Fuel cells are electrochemical devices that convert the chemical energy of fuels into electrical energy. An ideal option for a wide variety of portable, stationary, and automotive applications is using the polymer electrolyte
fuel cells due to their modular design, high efficiency, and environmental benefits.

A 3D microstructure of the non-woven gas diffusion layers (GDLs) of polymer electrolyte fuel cells (PEFCs) is reconstructed using a stochastic method. For a commercial GDL, ... Read more

Three dimensional (3D) composites were proposed over 40 years ago in an attempt to overcome the shortcomings of 2D laminates, by incorporating fibres into the through-thickness direction. 3D weaving offer significant manufacturing benefits as well as creating versatile textiles having a range of 3D architectures.

The development of fatigue damage in a glass fibre modified layer-to-layer three dimensional (3D) woven composite has been followed by time-lapse X-ray computed tomograp... Read more

Carbon capture and storage (CCS) offers a possible solution to curb the CO₂ emissions from stationary sources in the coming decades, considering the delays in shifting energy generation to carbon neutral sources such as wind, solar and biomass.

The most mature technology for post-combustion capture uses a liquid sorbent, amine scrubbing. However, with the existing technology, a large amount of heat is required for the regeneration of the liquid sorbent, which... Read more

Mass transport can significantly limit the rate of reaction and lead to concentration polarization in electrochemical devices, especially under the conditions of high operating current density.

In this study we investigate hierarchically structured micro-tubular solid
oxide fuel cells (MT-SOFC) fabricated by phase inversion technique and quantitatively assess the mass transport and electrochemical performance improvement compared to a conventional tubular SOFC. We present pioneer... Read more

This study aims to correlate the active triple phase boundaries (TPBs) to the variation of as-prepared anode microstructures and Ni densifications based on the reconstructed 3D volume of an SOFC anode, providing a point of comparison with theoretical studies that reveal the relationship of TPBs and the material microstructure using randomly packed spheres models.

Nickel/zirconia-based nanostructured electrodes for solid oxide fuel cells suffer from poor stability even at intermediate temperature.

This study quantifies the electrochemical and microstructural degradation of nanostructured electrodes by combining 3D tomography, electrochemical impedance spectroscopy (EIS) and mechanistic modeling. For the first time, the electrochemical degradation of nanostructured electrodes is quantified according to the fractal nature of the three-phase bounda... Read more

A simple chemical bath deposition is used to coat a complex porous ceramic scaffold with a conformal Ni layer.

The resulting composite is used as a solid oxide fuel cell electrode, and its electrochemical response is measured in humidified hydrogen. X‐ray tomography is used to determine the microstructural characteristics of the uncoated and Ni‐coated porous structure, which include the surface area to total volume, the radial pore size, and the size of the necks between the pores.... Read more

The most common means of fabricating membrane electrode assemblies (MEAs) for polymer electrolyte fuel cells (PEFCs) involves a hot-press step. The conditions used to perform the hot-press impacts the performance and durability of the fuel cell.

However, the hot-press process is not essential for achieving operational MEAs and some practitioners dispense with the hot-press stage altogether by using a self-assembled approach. By performing the integration of the components in-situ durin... Read more

Multiphase flow in porous media is strongly influenced by the wettability of the system, which affects the arrangement of the interfaces of different phases residing in the pores.

We present a method for estimating the effective contact angle, which quantifies the wettability and controls the local capillary pressure within the complex pore space of natural rock samples, based on the physical constraint of constant curvature of the interface between two fluids. This algorithm is ... Read more

Ni-YSZ anodes for Solid Oxide Fuel Cells are vulnerable to microstructural damage during redox cycling leading to a decrease in the electrochemical performance.

• Quantification of redox damage by coupling 3D tomography, EIS and nanoindentation.
• YSZ fracture, Ni detachment and agglomeration led to irreversible mechanical damage.
• Ni nanoparticles obtained upon redox cycling improve electrochemical performance.
• Loss in TPB densi... Read more

Electrospun all-fiber flexible supercapacitor with nanofiber electrodes/separator.

• Increased graphitic degree with the addition of MnACAC and thermal decomposition.
• Enhanced capacitive performance with the addition of MnO.
• Quantified nanofiber alignment and increased bias with MnO over undoped fibers.
• FIBSEM tomography of nanofibers showing MnO disitribution in carbon nanofibers.

We present an all-fiber flexible supercapacitor with compo... Read more